Patterson, M. C. L. He, S. Fehrenbacher, L. L. Hanigofsky, J. Reed, B. D.
Appeared in:
Materials and manufacturing processes
Paging:
Volume 11 (1996) nr. 3 pages 367-379
Year:
1996-05-01
Contents:
Several compositions of HfC-TaC codeposited by chemical vapor deposition were evaluated for oxidation protection of graphite substrates. Oxyacetylene torch ablation tests with an O2, C2, H2, ratio of 4:1 were used to test the adherence and composition of the coating and resulting oxides, which were subsequently characterized by x-ray diffraction and scanning electron microscopy. The preferred HfC-TaC composition of 70:30 was used to fabricate a 25 lbf graphite fiber reinforced rocket thruster with a unique structural design. Thruster testing at NASA Lewis was performed at 0.520 MPa chamber pressure and 1650°C (3000°F) using a 6 to 7:1,02,:H2 fuel mixture; a uniform, adherent oxide layer was observed on the internal surface of the combustion chamber following the test.