Three-step synthesis from dialkyl ketone (R2C=O) with C60 gave C60(CR2)n [R = Me, Et, Pr, Bu, (CH2)5.; n = 1, 2]. The adducts were isolated by means of gel permeation chromatography, and the monoadducts were characterized by 1H and/or 13C NMR spectroscopies as a mixture of major [5, 6] and minor [6, 6] isomers. Their solubility and electrochemical properties were reported.
Uitgever:
Taylor & Francis
Bronbestand:
Elektronische Wetenschappelijke Tijdschriften
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