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  Synthesis of Crystalline ZSM-5 Type Zeolites Utilizing Primary Monoalkylamines 1. Characterization
 
 
Titel: Synthesis of Crystalline ZSM-5 Type Zeolites Utilizing Primary Monoalkylamines 1. Characterization
Auteur: Ozvatan, SUmer
YUrUm, Yuda
Verschenen in: Energy sources. Part A, Recovery utilization and environmental effects
Paginering: Jaargang 23 (2001) nr. 5 pagina's 475-485
Jaar: 2001-06-01
Inhoud: ZSM-5 zeolite samples have been produced using a primary monoalkyl amine, sodium silicate solution which had three different compositions as sources of silica, and aluminum sulphate, Al2(SO4)3.16H2O, as a source of alumina in the initial gel. Crystalline ZSM-5 samples were produced using both technical grade and laboratory grade sodium silicate solutions. Product yields of the highly crystalline ZSM-5 samples obtained using technical and laboratory grade sodium silicate solutions were 74% and 60%, respectively. The highest crystalline products were obtained when using n-propylamine and n-butylamine as templates. Crystallinity increased as the reaction time also increased. In experiments using i-butylamine moderate crystallinities and yields, about 60% could be obtained. X-ray diffraction and FTIR methods have been used for the characterization of synthesized ZSM-5 zeolites.
Uitgever: Taylor & Francis
Bronbestand: Elektronische Wetenschappelijke Tijdschriften
 
 

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