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Details for article 8 of 10 found articles
| Title: | |
| Author: | |
| Appeared in: |
Analytical letters |
| Paging: | Volume 1 (1967) nr. 3 pages 201-211 |
| Year: |
1967 |
| Contents: |
The silylation of hydroxysteroids has been studied with different silylating reagents, and under non-catalyzed and catalyzed conditions. When BSA alone is used (non-catalyzed reaction), TMSi ether formation does not occur for 11β- and tert-17α-hydroxyl groups. When BSA-TMCS is used (catalyzed reaction), 11β-hydroxyl groups are converted to-TMSi ethers, and tert-17α-hydroxyl groups of the THE-THF series will also react. Complete silylation of all hydroxyl groups for compounds of the cortol series may be effected with TSIM-BSA-TMCS at 60° C. |
| Publisher: |
Taylor & Francis |
| Source file: |
Elektronische Wetenschappelijke Tijdschriften |
Details for article 8 of 10 found articles
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